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Old 15th September 2022, 12:04 PM   #1
JBG163
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The best way to know would be to have it polished and etched. The difference of color would be blatant. I supposed earlier that it could be quench but, more test would be necessary to be perfectly sure.

Still, keeping it in his current state is also a good thing. Especially for datation. It's all a balance and up to you asterix.

My knowledge in Kriss isnt deep enough to assess a revival style. So i entirely relay on Kai for his datation

An impressive sword in any case
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Old 15th September 2022, 12:23 PM   #2
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Originally Posted by JBG163 View Post
The best way to know would be to have it polished and etched. The difference of color would be blatant. I supposed earlier that it could be quench but, more test would be necessary to be perfectly sure.

Still, keeping it in his current state is also a good thing. Especially for datation. It's all a balance and up to you asterix.

My knowledge in Kriss isnt deep enough to assess a revival style. So i entirely relay on Kai for his datation

An impressive sword in any case
I forgot that it was you that originally posited the quench-line theory- thanks for that again, and also for your kind words!

I'll be doing an FeCl etch in the near future- I'll update this thread by then with clear and close-up pics
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Old 15th September 2022, 02:54 PM   #3
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I forgot that it was you that originally posited the quench-line theory- thanks for that again, and also for your kind words!

I'll be doing an FeCl etch in the near future- I'll update this thread by then with clear and close-up pics
No need to clair i'm first or not . Just couldnt be sure with the current state.
If you plan to etch, a good préparation would probably be requiered as the bottom of the blade looks quite pitted.

Kai, do you have encountered any exemple with a quench line like this ?
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Old 15th September 2022, 08:51 PM   #4
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Hello Julien,

Quote:
Kai, do you have encountered any exemple with a quench line like this ?
Not that I can remember, not that crisp and all over the blade, i believe.

And regarding the dating: As said, it's more of a hunch and needs serious research.

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Kai
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Old 16th September 2022, 01:53 AM   #5
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Hello Xas,

Quote:
I'll be doing an FeCl etch in the near future- I'll update this thread by then with clear and close-up pics
I'm not a big fan of ferric chloride - etching with it tends to be quite brutal to the surface and it's acting so fast that fine structures tend to be missed.

If you intend to polish the blade anyway, a quick & dirty exploratory etch with FeCL3 could help to show some details before you start the actual polishing.

You need a good polish to reveal finer structures. And a gentle/slow metallurgical etch to bring out the details without dulling the surface. Arsenic trioxide used in a traditional rub-on fashion works as do a number of more available modern etchants. I'd probably lean towards warm sodium persulfate; I can't claim to have tested most etchants though - doing this side by side on a representative test piece is still on my ever-growing to do list.

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Kai
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Old 19th September 2022, 06:07 PM   #6
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Arsenic trioxide used in a traditional rub-on fashion works as do a number of more available modern etchants.
Correct me if i am wrong here, but from my understanding arsenic trioxide isn't an etchant at all. It's function when used in the warangan mixture to stain a keris is that it turns iron and steel black while not effecting nickelous material in the pamor. That is how it raises the pamor pattern. It is the acid in the lime juice part of the mixture that acts as a gentle etchant.
I don't really know what causes the lines to appear in a twist core Moro kris, but if it is not the inclusion of nickel in the mix i don't think arsenic would be an effective way to raise the appearance of the lines in the twist.
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Old 19th September 2022, 09:31 PM   #7
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But an etchant would bring out the quench. And you would see a difference between the quenched zone and the "unquenched" one
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Old 19th September 2022, 11:41 PM   #8
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An xray might be interesting to see. Know anyone who works in a hospital or Dentist's office?
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Old 20th September 2022, 02:47 AM   #9
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Hello Rick,

Quote:
An xray might be interesting to see. Know anyone who works in a hospital or Dentist's office?
From the pamor extending across the line, it seems safe to assume that we don't see any differences on a macroscopical level here. Thus, I don't think x-ray will be of any help here.

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Kai
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Old 20th September 2022, 02:50 AM   #10
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Hello Julien,

Quote:
But an etchant would bring out the quench. And you would see a difference between the quenched zone and the "unquenched" one
Yes, any difference in final composition (steel alloy, heat treatments, etc.) will show up by etching/staining.

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Kai
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Old 20th September 2022, 03:05 AM   #11
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Hello David,

Quote:
Correct me if i am wrong here, but from my understanding arsenic trioxide isn't an etchant at all. It's function when used in the warangan mixture to stain a keris is that it turns iron and steel black while not effecting nickelous material in the pamor. That is how it raises the pamor pattern. It is the acid in the lime juice part of the mixture that acts as a gentle etchant.
Yes, I was referring to the traditional mixture of arsenic with lime juice. And, for brevity, I wasn't differentiating between etching and staining.

Any etching/staining result will not only be affected by the steel alloys (possibly containing different amounts of nickel, phosphorous, etc.) but as well from differences in heat treatment, especially quenching.


Quote:
I don't really know what causes the lines to appear in a twist core Moro kris, but if it is not the inclusion of nickel in the mix i don't think arsenic would be an effective way to raise the appearance of the lines in the twist.
In most cases, Moro "twistcore" blades will have been crafted from layering mild steel and another steel with noticeable nickel content (probably from Luwu?), indeed.

Regards,
Kai
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Old 20th September 2022, 03:33 PM   #12
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Originally Posted by kai View Post
Hello David,


Yes, I was referring to the traditional mixture of arsenic with lime juice. And, for brevity, I wasn't differentiating between etching and staining.

Any etching/staining result will not only be affected by the steel alloys (possibly containing different amounts of nickel, phosphorous, etc.) but as well from differences in heat treatment, especially quenching.



In most cases, Moro "twistcore" blades will have been crafted from layering mild steel and another steel with noticeable nickel content (probably from Luwu?), indeed.

Regards,
Kai
Well Kai, i think you really have to differentiate between etching and staining because they are not the same thing at all. Actually i don't think all that much etching takes place during the staining process with warangan anyway. Most of the etching with keris takes place during the pre-staining "cleaning" processes when either fruit acids or coconut water are used to remove rust and bring the blade to "whitened" condition.
I was not arguing that there is not nickel in the steel of this archaic Moro blade. But by my understanding the patterns created here are not done by the same process that is used to create keris with pamor. There is not pamor used in this archaic blade as far as i know. There may very well be some nickel content in some of the iron used though. But frankly i don't know. I am curious to know how you know this though. Can you cite a source for this information?

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Old 8th February 2023, 11:33 PM   #13
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Hello David,

Apologies for not responding earlier!

Quote:
Well Kai, i think you really have to differentiate between etching and staining because they are not the same thing at all.
In most cases of intentionally treating pattern-welded pieces, both is happening during a single process like two sides of the same coin.

Pretty much all stains contain an acid which etches the surface and some resulting oxidation products result in discoloration of the bare metal.


Quote:
Actually i don't think all that much etching takes place during the staining process with warangan anyway. Most of the etching with keris takes place during the pre-staining "cleaning" processes when either fruit acids or coconut water are used to remove rust and bring the blade to "whitened" condition.
Yes, the whitening step is responsible for most of the erosion, especially with the rub-in method. (The soaking method tends to remove more metal.)

However, the lime juice in the warangan mix provides organic acids resulting in an oxidation process while the arsenic reacts resulting in the dark color. Thus, we still have both processes working hand in hand (since the lime juice is necessary to get a correct stain).


Quote:
I was not arguing that there is not nickel in the steel of this archaic Moro blade. But by my understanding the patterns created here are not done by the same process that is used to create keris with pamor.
Pamor can result from any kind of laminations, even if the contrast happens to be low. Also in Indonesian keris, the use of metal from different ores/treatments results in obvious (if often more subdued) laminations, especially with many old pieces. If the ores don't have increased nickel content, it may just as well be a higher phosphorus content or other trace element(s) in the alloy affecting their specific reaction characteristics.


Quote:
There is not pamor used in this archaic blade as far as i know.
This example clearly exhibits typical pamor (easily comparable due to the smooth surface) of the same twisted type as seen on keris Jawa (or Lombok/Bali). Based on the thin pamor layers with very light color, I'm pretty confident that a XRF analysis will show an elevated percentage of nickel in this blade, indeed.


Quote:
There may very well be some nickel content in some of the iron used though. But frankly i don't know. I am curious to know how you know this though. Can you cite a source for this information?
If it walks like a duck, and quacks like a duck...

At this stage, I don't have really started obtaining detailed measurements yet (quite tricky due to the small exposed surfaces, especially with more complex pattern-welded blades).

Aside from originating from the same roots, also all observed features resulting from blade forging and quenching as well as the very comparable reaction of pamor layers to etchant/stains, supports the hypothesis that at least the basic keris/kris smithing methods seem to be very similar all across the archipelago.

Regards,
Kai
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Old 8th February 2023, 09:26 AM   #14
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I forgot that it was you that originally posited the quench-line theory- thanks for that again, and also for your kind words!

I'll be doing an FeCl etch in the near future- I'll update this thread by then with clear and close-up pics
Hello Xasterix, I was wondering wether you ever followed up with a FeCl treatment.

I am thinking of asking a blacksmith to do this with my Moro Maguindanao Kris and wanted to see what the effects are. I don't have the facilities to do this myself. How, if you did, did you you go about protecting the hilt from the FeCl?


I look forward to see your answer hoping that you get an alert from the forum after my quoting your post from last year
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Old 8th February 2023, 04:23 PM   #15
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Hello Milandro,

As mentioned above (post #21), I'm not favouring etching with ferric chloride. The stain will often exhibit pretty warm colors (i.e. rusty), sometimes after some time only.

Even if one has experience in its use on modern pattern-welded blades, there is a chance that leftover chloride ions will keep nagging on a blade, especially with antique blades that are more likely to have crevices from cold shuts, eroded surfaces, etc.

Pretty much all Moro aficionados are nowadays utilizing warm diluted acetic acid. While the resulting pattern will be more subdued, it certainly seems close enough to what real user blades probably looked like.

Regards,
Kai
(BTW, I see that I failed to answer David's post - will do ASAP)

Last edited by kai; 8th February 2023 at 10:27 PM.
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Old 8th February 2023, 05:16 PM   #16
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Cheers Kai,

I realise that the topic of staining is controversial .

Since I have never seen a Kris blade (Moro or otherwise) which has been stained with FeCl, I took the chance offered in this thread to see how one would have looked like.

Since Xasterix announced the staining (staining which was " to come" at that time) of this blade in FeCl and the intention to post pictures as a follow up : ".... I'll be doing an FeCl etch in the near future- I'll update this thread by then with clear and close-up pics ..."

I was wondering if this had happened and if we could partake of the results.

I have seen several pictures of blades stained in vinegar and, for comparison, would be very educative and informative for all to see the difference between the two (of course , Ideally one would have to see it on the same blade but also two similar one would be the next best thing)

Last edited by milandro; 9th February 2023 at 08:31 AM. Reason: syntax
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Old 8th February 2023, 10:32 PM   #17
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Yes, I may be the culprit in dissuading Ray to move forward...

We had some Moro blades treated with ferric chloride here in the forum (if not findable with a search, possibly in the defunct UBB forum). I'm going to PM you examples that I can't post here, Milandro.

Regards,
Kai
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Old 9th February 2023, 01:57 AM   #18
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Quote:
Originally Posted by kai View Post
Yes, I may be the culprit in dissuading Ray to move forward...

We had some Moro blades treated with ferric chloride here in the forum (if not findable with a search, possibly in the defunct UBB forum). I'm going to PM you examples that I can't post here, Milandro.

Regards,
Kai
Here's one Kai.
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Old 9th February 2023, 10:10 AM   #19
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Hullo Milandro! Sorry it took me a while to get back. I didn't FeCl the kris anymore. As chance would have it, I was able to contact a descendant-relative of the original Maguindanaon owner, and upon realizing the value of that pusaka, they expressed that they would like to acquire it in memory of their ancestral lineage. As much as I want to keep it (who won't want to keep a twistcore, right), out of goodwill I let them acquire it from me. That's one less twistcore for me, but at least a family reclaimed its pusaka.

Anyhow- I've been experimenting a bit, and my current preference is a mix-
1. Mirror polish then FeCL, stabilize
2. I immerse a white vinegar-filled tube with old brass for around 2 hours
3. I dip the blade for around 30 mins (as a second etch), stabilize

So far I'm pleased with the results. It doesn't show up that clearly in my pics, but there's a golden tone to the etch in certain places (due to the brass residue). Here's some pieces I did that progression with.
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Old 9th February 2023, 01:50 PM   #20
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Hello Xasterix,

thank you very much for getting back to this thread with such relevant information and very well done for returning the acquired kris to the family of the original owner. You are a gentleman.

Anyway.

Thanks for sharing your experience and your personal recipe.

I am considering all options for my one Moro blade (which I did publish elsewhere in another thread but I can add a picture here for completeness of the discussion).

I don't think it has a twist core or any other major feature , yet, I think that giving it the chance to show the hidden secrets (so to speak) may be a nice touch.

I am going to consult a local master bladesmith , hoping that he can provide some insights from a " de visu" exam of the blade.
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Old 9th February 2023, 08:44 PM   #21
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As chance would have it, I was able to contact a descendant-relative of the original Maguindanaon owner, and upon realizing the value of that pusaka, they expressed that they would like to acquire it in memory of their ancestral lineage. As much as I want to keep it (who won't want to keep a twistcore, right), out of goodwill I let them acquire it from me. That's one less twistcore for me, but at least a family reclaimed its pusaka.

2. I immerse a white vinegar-filled tube with old brass for around 2 hours
It’s honorable of you to have the Maguindanaon family have their Pusaka back.

What’s the purpose of adding the brass to the vinegar?
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